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简介：报道了采用温控氢电弧法制备C60及C70。未须纯化，采用透射电镜可直接观察到C60及C70的微观晶体结构。虽然该法产量较低，但为制备C60及C70提供了一种新方法。

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简介：Themicrostructureofthelasermelted1.0%Ctoolsteelhavebeeninvestigated.Theregionaffectedbythelasercanbesubdividedinto3zones,whichconsistofameltedregionatthesurface,azonewithsolidstatetransformationandtheareaadjacenttotheunaffectedsubstratewherecementiteisslightlydissolved.Themeltedzonepossessedacellulargrowthmorphologyconsistingofausteniteandmartensite.Thecarboncontentoftheaustenitewasmeasuredtobeover1wt-%.Agreatdealofretainedausteniteandtwinnedmartensitewerefoundinthefirsttwozones(themeltedandsolidtransformed).

简介：美国Nucor公司报道，他们利用Castrip工艺首次完成累计10万t的生产大关，薄钢板设计厚度在0．7～2mm范围内。

简介：Defectsofpolymer-derivedSi-C-OfiberswereintensivelystudiedbytheSEMandTEMtechniquesandtheiroriginationswerealsodiscussedonthebasisoffactorsexperiments.Thedefectswerefoundmainlyintheformofstrumaes,pitsandsplitsonsurfacesaswellasmicroflawnetworks,porosityclustersandinclusionsinthebulk.Factorsexperimentsrevealthatanonuniformoraninsufficientcuringwouldresultinlarger-sizedstru-maesorinteriormicroflaws.Gasevolutionratesduetodifferentfiringrateshaveagreatinfluenceontheformationofinternalmicrofiawsorporosityclustersandsomeoxidation-inducedpitsorsplitsmaybeformedonsurfacesbe-causeoratraceofoxygenorwatervaporaccumulatedfromtheflowinginertatmosphereduringpyrolysis.

简介：采用扩展的Huckel方法与格林函数方法，分析了双Au电极作用下C60富勒烯分子的电子结构与电子输运特性。研究结果表明，C60富勒烯分子与Au电极“接触”后，其分子轨道能级发生了较大的变化，HOMO、LUMO间的能隙显著减小；C60与Au电极之间的结合既有共价键的成分，又有离子键的成分；C60富勒烯分子的电压-电导率曲线以及伏安曲线表现出了微妙的量子特性。

简介：据媒体报道，由中国农业科学院麻类研究所等单位合作开展的麻类等纤维质预处理、糖化液酵解生成燃料乙醇研究，取得重大突破。其麻类等纤维质酶降解生产燃料乙醇技术己于近日通过国家级鉴定。

简介：Basedontheclassicdiffusioncontrollednucleationandgrowththeory,thesympatheticnucleationledgewisegrowthmechanismofbainitewasstudiedtheoreticallyforIowcarbonFe-Calloys.Therationalityoftheoccurrenceofsympatheticnucleationontheterracesofledgescompetingwithlateralledgegrowthandothersitesnucleationwasdemonstratedbythepresentworkquantitatively.ThecalculationsindicatedthatIowreactiontemperaturesandhighcarbonconcentrationsmayfavorthesympatheticnucleation,thusaccountingfortheformationofmultilayerstructuresofbainite.

简介：TheRamanspectraof3%(molefraction)Y2O3-ZrO2(3Y)areobtainedatdifferenttemperaturefrom77Kto853K.Theresultsshowthat260cm-1Egand460cm-1Egmodesonthespectrashifttowardlowerwavenumberwiththeincreaseoftemperature;meanwhile,thecontinuityoftheHalfWidthatHalfMaximum(HWHM)andwavenumber(frequency)ofRamanbandsarebrokenandt-phaseonlypartiallytransformstom-phaseat523K.Basedontheexperimentalresults,thispaperdiscussesthet-phaselatticevibrationof3YandpresentstheimagesofvibrationdisplacementofsixRaman-activemodesfort-phaseofZrO2.TheanalysisindicatesthattherearediversitiesexistinginthedisplacementoftheatomicvibrationofRaman-activemodesbecauseoftheirdifferentsymmetriesatvarioustemperature,whichleadstothedifferentchangetendenciesofRamanbands.Furthermore,theabruptchangesofsomeRaman-activemodesindicatingtheatomicdisplacementareassumedtobethecondensationsofphononmodesinthet→mphasetransition.

简介：Sodiumparanitrophenolatedihydrate(NPNa·2H2O)isanexcellentsemiorganicnonlinearoptical(NLO)material,crystallizesbothinwaterandmethanolwithhighdegreeoftransparency.Goodopticalqualitysinglecrystalsofdimensionupto18mmx6mmx3mmareobtainedbyisothermalsolventevaporationtechnique.Thesolubilityofthecrystalindifferentsolventswasmeasuredgravimetrically.ThesinglecrystalsofNPNa·2H2Oshowvariationinphysicalpropertiesandgrowthrateindifferentsolvents.Methanolorethanolsolutionyieldscrystalsofbipyramidalshapewithclearmorphology.However,methanolgrowncrystalisexhibitingimprovedhardnessparametersandpossessesexcellentthermalstabilityascomparedtowatergrowncrystals.TheeffectsofsolventonhardnessparameteralongwiththermalandopticalpropertiesofNPNa·2H2Owasrevealedinthispaper.