简介:Al-5Ti-0.5C-8Sr(集体部分,%)主人合金用一个melt反应方法被准备。微观结构和主人合金的合成过程被光显微镜学,X光检查衍射,扫描电子显微镜学和X光检查调查精力散的光谱。结果证明主人合金由组成一(艾尔),TiAl3,TiC,Al4Sr和Al-Ti-Sr分阶段执行。主人合金的合成机制如下:TiAl3通过在K2TiF6和艾尔之间的反应被形成在基础材料的部分融化层融化在850个C粒子与同类地分布式的加强在超声的行动和一张契约下面被变成液体filler在团结以后被获得。体积部分原文如此,在契约的粒子能被改变以铜锌金焊接的温度改变。最大值原文如此,契约材料的粒子体积部分在brazi到达了37%?
简介:ThesubmicronpowdermixturesofTiC-TiN-WC-Mo-C-Nisinteredat1400℃orbelowinvacuumwerestudiedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM)andtransmissionelectronmicroscopy(TEM)analyses.TheresultsshowedthatMo2Cformedat800℃orbelow.BothWCandMo2Cdisappearedat1200℃,andTiNdisappearedat1250℃.Inaddition,thevariationsoflatticeconstantsofthetitaniumcarbonitrideandnickelbinderphasewithsinteringtemperaturewereexperimentallyobtained,andthereasonwasanalyzed.
简介:采用选晶法在真空定向凝固炉中,制备了C含量分别为0.019%、0.048%、0.074%和0.094%的单晶高温合金,合金表面吹沙后分别在1250、1300℃进行真空热处理,研究不同C含量对单晶高温合金再结晶的影响。结果表明:随着合金中C含量升高,碳化物含量增多,其形态由块状转变为骨架状、发达骨架状;随着C含量增加,合金再结晶层深度无明显变化趋势,这表明碳化物对合金再结晶无明显的抑制作用,随着热处理温度升高,再结晶厚层深度明显增加;C对单晶高温合金再结晶抑制作用与形成碳化物的形态和密度有关,在合金表层形成高密度的碳化物,从而对再结晶晶界形成钉扎作用,阻碍晶界的迁移,能够起到抑制再结晶的作用。
简介:Three-dimensionalfiniteelementmodelwasestablishedtosimulatetemperaturefieldsofT-jointtitaniumsheetsduringTIGweldingwithfiniteelementmethod(FEM)software.Temperaturedependentmaterialpropertiesandtheeffectoflatentheatwereconsidered.Atechniqueofelementbirthanddeathwasusedtosimulatetheprocessofweldedmetalfilling.DynamicvariationprocessoftemperaturefieldsduringTIGweldingwasachieved.Thesimulatedresultsagreedwellwiththemeasuredresults.
简介:Inthisstudy,atwo-stepheatingprocessisintroducedfortransientliquidphase(TLP)diffusionbondingforsoundjointswithT91heatresistantsteels.Atfirst,ashort-timehighertemperatureheatingstepisaddressedtomelttheinterlayer,followedbythesecondsteptocompleteisothermalsolidificationatalowtemperature.Themostcriticalfeatureofournewmethodisproducinganon-planarinterfaceattheT91heatresistantsteelsjoint.WeproposeatransitionalliquidphasebondingofT91heatresistantsteelsbythisapproach.Sincejointmicrostructureshavebeenstudied,wetestedthetensilestrengthtoassessjointmechanicalproperty.Theresultindicatesthatthesolidifiedbondmaycontainaprimarysolid-solution,similarcompositiontotheparentmetalandfreefromprecipitates.Jointtensilestrengthofthejointisnotlowerthanparentmaterials.Jointbend'sstrengthsareenhancedduetothehighermetal-to-metaljunctionproducinganon-planarbondlines.Nevertheless,thetraditionaltransientliquidphasediffusionbondingproducesplanarones.Bondingparametersofnewprocessare1260℃for0.5minand1230℃for4min.
简介:Themicrostructureandmechanicalpropertiesoffrictionstirwelded2.5mm7050-77451aluminumalloynaturalaging72hand17520hwereinvestigated,respectively.Theuniaxialtensiletestshowedthatyieldstrength,tensilestrengthandelongationofthejoints17520hnaturalagingwereabout20%,12%and24%higherthanthosejointsnaturalaging72h.Hardnessprofileofnaturalaging17520hjointwitnessedsignificantenhancementinnuggetzone,comparedwith72hnaturalaging.Differentialscanningcalorimetry(DSC)andtransmissionelectronmicroscopy(TEM)testrevealedthatmoreGuinier-Prestonzone,η'andηphaseemergedinnuggetzoneasnaturalagingdurationincreased,highdensityofdislocationlocatedwithingrainboundaryinnuggetzoneofjointsnaturalaging72h.ItisconcludedthatnaturalagingwasfeasibletoenhancestrengthandplasticityofFSWjointssimultaneously.
简介:以MoO3粉、Mo粉、Si粉及Al粉为原料,采用机械合金化法合成了纳米Mo5Si3-20%Al2O3(质量分数)复合粉体。采用XRD、SEM、TEM和DTA等对复合粉体在球磨过程中结构变化进行了研究。结果表明:球磨10h后合成的Mo5Si3-20%Al2O3复合粉体,反应以爆炸模式进行。球磨30h后,Mo5Si3和Al2O3的晶粒尺寸分别为36.3nm和21.9nm。随着球磨时间的延长,Mo5Si3和Al2O3的晶粒尺寸变小,衍射峰宽化程度降低。DTA和XRD分析结果表明,复合粉体具有好的热稳定性,球磨30h后再在1000℃退火1h后复合粉体没有发生物相转变。更多还原