简介:采用喷雾干燥-氢气还原法制备出W-20wt%Cu超细复合粉末,并对由该复合粉末所制得的压坯进行了高温烧结,利用SEM、XRD等分析手段对复合粉末的特性和烧结体的组织进行了表征和观察。实验结果表明,由该方法制备的W-20wt%Cu超细复合粉末颗粒细小,平均粒径在200nm左右;喷雾干燥后的氧化物复合粉末在还原后产生了新的合金相(Cu0.4W0.6),还原后的复合粉末由Cu0.4W0.6相和Cu相组成,而且两相的晶粒度达到纳米级,其中Cu0.4W0.6相的晶粒约为33nm,Cu相的晶粒约为63nm;复合粉末具有很高的烧结特性,经高温烧结后合金致密度达到98%以上,而且金相组织分布均匀。
简介:AnumericalmodelAlloy/MhasbeenappliedtoinvestigatethemicrosegregationinAl-4.45wtpctCualloy.Thecalculateddatawerecomparedwiththeexperimentalmeasurementsforsamplessolidifiedatdifferentcoolingrates.Discrepanciesinsoluteconcentrationoccurbetweentheexperimentalobservationsandcalculatedresults.Reasonsforthediscrepancieswerediscussed,andtheeffectofdendritejoiningatalaterstageofsolidificationonthemicrosegregationwasinvestigated.Calculationsthathaveincludedthiseffectshowedabetterfitwithexperimentalresults.
简介:在团结微观结构的谷物结构和precipitates极端纯有不同Ti或Nbmicro-alloying的17wt%Cr以铁酸盐为主要成的不锈钢试验性地并且理论上被调查。到钢的Ti或Nb的增加减少了谷物尺寸(D)和延伸因素(E),这被谷物结构观察发现,并且改进了equiaxed谷物比例(P)和球状因素()。在学习的四钢之中,最小的谷物尺寸和最大的equiaxed谷物比例被联合把Ti和Nb加到钢获得。SEM观察显示了那几种猛冲例如锡,MC(在Nb的富人),等等,洗阶段(Fe2Nb)在相应的钢形成了。另外,用Thermo计算软件计算的结果说明了那听在合适的Ti和N内容在液体猛抛。同时,团结间隔(T)被Ti或Nb的增加扩大,并且Nb的有效性比Ti强壮。基于试验性并且计算结果,在equiaxed谷物比例的谷物精炼和增长的机制被讨论。
简介:目前家居无线宽带保障安全的方法,不外乎加装防火墙,购买杀毒软件和在路由器上进行安全设置,这些方法已经被证明行之有效。而笔者最近发现了一款由趋势科技与合勤科技合作开发的新一代家居无线宽带路由器ZyXELP-334WT。它捆绑了趋势科技的防毒软件,这无疑又是一个软硬结合保障家居无线宽带安全的范例。该款产品造型为银色镜面,搭配黑色的外壳及天线,内建六国语言设定接口。它提供了无线“g+SuperSpeed”技术和宽带安全服务(TrendMicroHomeNetworkSecurityDervices,TMSS系统),可以帮助用户建立严密的家居网络防护体系。
简介:TheW-Cucompositesarewidelyusedasweld-ingelectrodes,electronicpackagingmaterials,electricdischargematerialsandheatsinksbecauseoftheexcellentproperties.Inthisresearch,theW-40wt.%Cucompositeswerepreparedthroughthevacuumhot-presssinteringmethod,andtheeffectofsinteringtemperatureonthemicrostructureand
简介:Inthisarticle,anovelheattreatmentmethod,deformationheat(DH)treatment(extrusion+aging),wasemployedonahypereutecticaluminumsiliconalloy(LM28-0.3wt.%Nd),anditseffectonmicrostructureandmechanicalpropertiesofthisalloywasinvestigated.ItcanbeconcludedthattheeutecticmicrostructuredisappearsaftertheDHtreatment,inthemeantimethemorphologyofα(Al)solidsolutionwastransformedfromfir-treeandcellulartoequiaxed,Siwasrefinedwithgrainsizesofabout1-10μmanddistributeddispersedly,evensomeofthembecameglobularshape,whichcanreducestressaccumulationeffectively.MechanicalpropertiestestindicatedthattheDHtreatmentcouldsignificantlyimprovetheroom-temperaturestrengthandhavelittleeffectonthehigh-temperaturestrengthofLM28-0.3wt.%Ndalloy.Thefracturemechanismisductilefracturebyfracturemorphologyanalysis.
简介:目的检测WTI和P53在卵巢浆液性肿瘤中的表达,探讨其临床病理学意义及二者的关系。方法采用免疫组化Envision二步法检测在卵巢良性浆液性肿瘤、交界性浆液性肿瘤和浆液性癌各40例中的WT1和P65表达情况,分析其表达水平与卵巢浆液性癌中临床病理特征的关系。结果WT1在卵巢良性浆液性肿瘤、交界性肿瘤和浆液性癌中阳性表达率分别为22.5%、72.5%和90%(P〈0.05),差异均有统计学意义。P53在卵巢良性浆液性肿瘤、交界性肿瘤和浆液性癌中阳性表达率分别为7.5%、27.5%、75.0%,差异有统计学意义。结论WT1和P53可能参与了卵巢浆液性肿瘤的发生发展。
简介:TheslidingfrictionandwearbehaviorsofMg–11Y–5Gd–2Zn–0.5Zr(wt%)alloywereinvestigatedunderoillubricantconditionbypin-on-diskconfigurationwithaconstantslidingdistanceof1,000minthetemperaturerangeof25–200°C.Resultsindicatethatthevolumetricwearratesandaveragefrictioncoefficientsdecreasewiththeincreaseofslidingspeeds,andincreasewiththeincreaseoftesttemperaturebelow150°C.ThehardandthermallystableMg12(Y,Gd)Znphasewithlong-periodstackingorderstructureinthealloypresentssignificantwearresistance.Thewearmechanismbelow100°Cisabrasivewearasaresultofplasticextrusiondeformation.Thecorporateeffectsofsevereabrasive,oxidative,anddelaminatingwearresultinthetribologicalmechanismabove100°C.
简介:InordertoimprovethecorrosionandmechanicalpropertiesofAM50magnesiumalloy,1wt.%GdwasusedtomodifytheAM50magnesiumalloy.Themicrostructure,corrosionandmechanicalpropertieswereevaluatedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),energydispersivespectroscopy(EDS),electrochemicalandmechanicalstretchmethods.Theresultsindicatedthatβ-Mg17Al12phasedecreasedandAl2Gd3andAl0.4GdMn1.6phaseexistedafterGdaddition.BecauseoftheGdaddition,thegrainofAM50magnesiumalloywasrefinedsignificantly,whichimprovedthetensilestrengthofAM50magnesiumalloy.Thedecreasingofβphaseimprovedthecorrosionresistanceofthemagnesiumalloy.ThefracturemechanismoftheGdmodifiedAM50magnesiumalloywasquasi-cleavagefracture.Thecorrosionresidualstrength(CRS)ofAM50magnesiumalloywasimprovedafter1wt.%Gdaddition.