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简介：Thecrackingandaromatizationofn-hexaneoverH-ZSM-5modifiedbyvariousrareearthswereinvestigatedbymeansofcontinuousflowmicro-reactor.ThesurfacepropertiesofmodifiedH-ZSM-5catalystswereobtainedfromIR,XRDandXPS.Theresultsshowthattherareearthsenhancethearomatizingpropertiesofthecatalystswhicharepreparedbymechanicalmixturemethod.Theresultsofn-hexanecrackingandaromatizationarecorrelatedwiththeacidity.TheBrnstedacidicsitesaretheactivesitesofn-hexanearomatization,whileLewisacidsiteplaysanimportantroleinn-hexanecracking.

简介：Silicawasused,asacatalystcarrier,toloadceroussulfateforcatalyzingthesynthesisofn-butylacetate.Themainpurposeofthisresearchwastoexplorethefeasibilityofsilicainimprovingthedecentralityandactivityofthecatalyst.Theeffectsofmolarratioofbutylalcoholtoaceticacid,theceroussulfateloadingsandthereactiontimeontheconversionofaceticacidwerestudiedbysinglefactorexperimentmethodandorthogonalexperimentmethodrespectively.Therefractiveindex(n20D)andmolecularstructureofthepreparedn-butylacetateweremeasuredbyAbbeRaefractometerandFourierTransformInfraredspectroscope,respectively.Thecomparisonsofthesilicaloadedandunloadedcatalystsforcatalyzingthesynthesisofn-butylacetateweremade.Theresultsshowedthatthesuitableconditionsforsynthesizingn-butylacetatewere:molarratioofbutylalcoholtoaceticacidof1.4∶1,uselevelofloadedceroussulfateof0.30gandreactiontimeof50min,respectively.Themaximumconversionofaceticacidforthesilicaloadedcatalystreached98.62%whichwas12.32%and16.43%higherthanthosefortheunloadedcatalystsreportedinliteratures,buttheuselevelofceroussulfatefortheformerwasmuchlessthanthoseforthelattersundersimilaroptimaltechnicalconditions.Thesilicawasprovedtobeagoodcatalystcarrierforenhancingdecentralityandactivityofthecatalystandincreasingtheconversionofaceticacid.Therepentanceofthesilicaloadedceroussulfatewasalsoinvestigatedintheexperiment.

简介：SeveralREEdatasetswerecollectedinCoreDD2andEC2005intheinnershelfofEastChinaSea,CoreY127inthenorthernOkinawaTrough,CoreNT1,C9247andC92169inthesouthYellowSeatochecktheapplicabilityoftheδEuN-ΣREEsmodelforquantita-tivelydistinguishingsedimentsfromtheYangtzeRiverandtheYellowRiver.Bycomparison,severalsedimentsincoresDD2,EC2005,Y127aregenerallyinaccordancewiththismodel.ThecoresNT1,C9247andC92169,whichhavebeeninfluencedbytheYangtzeRiverandtheYellowRivertogether,however,wereinconsistentwiththeδEuN-ΣREEsmodel.TheδEuN-ΣREEsplotanditscorrespondingregressionequation,whichcouldbeusedtodistinguishsediments＂intuitivelyandquantitatively＂fromtheYangtzeRiver,andtheYellowRivershouldbereconsideredorreassessed.

简介：通过合理的成分设计,采用洁净钢冶炼工艺、两阶段轧制技术、热处理生产技术,成功的研制出符合客户要求的正火态热处理管线钢。通过性能检验,产品晶粒细小、组织均匀、性能富裕量较大,完全可以满足用户大批量供货要求。

简介：二高度光的铕(III)和铽(III)的准备有succinimide(SI)和N-hydroxysuccinimide(NHSI)的建筑群被报导，它进一步通过元素的化学分析，热分析，英尺红外，粉末X光检查衍射，SEM和荧光光谱学被调查。通过这些分析收集的数据揭示了Eu(III)的形成，有上面的Tb(III)建筑群对ligand在金属提及ligands(M:L)1:3的臼齿的比率。光中心从photoluminescent系列调查被保留的关于通过lanthanide的协作地点的有效促进感受性的有趣的结论。当时，强壮的光排放在Eu(III)-SI和Tb(III)-NHSI建筑群的情况下被观察-SI建筑群展出了的相应Eu(III)-NHSI和Tb(III)没有相片光性质。最新获得的光lanthanide建筑群可能具有为在光电子的各种各样的应用的特别兴趣。

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简介：采用理论计算与热分析相结合的方式对N08904超级奥氏体不锈钢的液相线温度进行了计算测试,提出了合理的过热度参数,解决了连铸易漏钢问题,实现了连铸生产。

简介：介绍了南钢开发E36N高强船板的主要技术思路和关键工艺控制。通过对炼钢工艺的严格控制，得到了较高纯净度、内部质量较好的连铸坯；通过微合金化、合理的控轧控冷和正火工艺，得到了组织较细化的E36N钢板，具有优良的综合力学性能，满足供货要求。

简介：利用某公司生产的精铋（4N）作为阳极，采用氟硅酸铋-氟硅酸溶液为电解液，进行精铋电解生产5N高纯铋试验。试验结果表明，以氟硅酸铋-氟硅酸溶液作为电解液，进行精铋电解能生产出5N高纯铋，解决了传统铋电解精炼过程中杂质铅难以除去的问题，为5N高纯铋的生产提出了一条新的可行途径。

简介：中厚板卷厂通过转炉终点碳含量控制，LF白渣精炼，RH真空脱气、钙处理，连铸机加强保护浇注，使用低碳保护渣生产低碳低阻钢，铸坯低倍情况良好，轧后性能符合要求。

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简介：Inthisstudy,aroll-bondedUNSN088225alloycladpipelinesteelwasinvestigatedanddevelopedinBaosteel.Basedontherequirementsofanumberofpotentialprojects,weperformedaseriesofstrictevaluationsincludingmechanicalandcorrosiontests.Theresultsshowthemechanicalpropertiesandcorrosionresistanceofthiscladsteeltobeexcellentandtomeettherequirementsofallthedesignparameters.

简介：通过对欧标S355J2+N中厚板正火实验研究,总结了正火温度、正火保温时间及不同轧制冷却工艺条件下对产品性能变化的影响,提出了对正火轧制产品的看法及建议。

简介：ThecausestotheoutersurfacefoldingdefectsinN80-Qoilcountrytubulargoods(OCTG)wereinvestigatedthroughtheobservationofthedefects’morphology,microstructureandtheanalysisofthechemicalcompositions.Itisbelievedthatthedefectwasresultedfromtheintrinsicflawsthatoriginallyexistedonthebillet;theywereextendedandoxidizedduringthefollowingreheatingandrollingprocesses.Withmorestrictqualitycontrolandinspectionofthebillet,thedefectcanbepreventedeffectivelyfromoccurring.

简介：TheFe-Ti-Nmateralloywaspreparedthroughthein-situreactionofnitrogengaswiththeFe-Timelt.ScanningelectronmicroscoperesultsshowthattheparticlesuniformlydistributedintheironmatrixwereTiN.ThedeliberatelypreparedFe-Ti-Nmasteralloywasemployedforthe409Lferriticstainlesssteelinanattempttorefinetheas-castsolidificationstructure.ItwasfoundthattheeffectivenessofFe-Ti-Nmasteralloyonrefiningoftheas-cast409Lferriticstainlesssteelwasaffectedbyadditionlevel,holdingtimeandmeltstemperature.Itwasfoundthattheaverageequiaxedgrainsizedecreasedfrom1503μmto303μm,theproportionofequiaxedgrainzoneincreasedfrom14%to100%withincreasingtheFe-Ti-Nmasteralloyadditionlevelto2.5%.Theproportionofequiaxedgraindecreasedfrom85%to4%asthesolidificationtemperatureincreasedfrom1803Kto1883K.Whentheholdingtimereachedto8min,thesolidificationstructuresof409Lferriticstainlesssteelshowextremepointsintheproportionofequiaxedgrain.Itisclearthatthegrainrefiningefficiencygraduallyfadeawaywiththeincreasingoftheholdingtimeattheverybeginning.However,whentheholdingtimecontinuestoincreaseandexceedstheextremepoint,thegrainrefiningefficiencyoftheFe-Ti-Nmasteralloyrecoveredtoacertaindegree.Theexperimentalresultsmentionedabovehavebeenanalyzedintermsofthermodynamics.Underappropriateconditions,theFe-Ti-Nmasteralloyusedforgrainrefinementofthesolidificationstructureof409Lferriticstainlesssteelmayhavegoodprospectsforindustrialapplications.

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简介：据报道，中科院病原微生物与免疫学重点实验室研究人员4月8日对记者表示，病毒片段重配研究结果显示，H7N9病毒的8个基因片段中，H7片段源于浙江鸭群中分离的禽流感病毒，

简介：介绍了奥氏体焊缝组织及薄板在超声波探伤检测应用的主要难点，描述了常规扫描成像超声检测方法和相控阵超声检测方法两种检测方法特点，针对生产的4mm厚纯镍N6板材焊接组织采用两种方法进行探伤检测试验，选定检测设备型号、焊接方法及焊接参数，按照检测要求制备试验试块。通过检测分析得出，常规超声检测方法在较好的条件下，仍然对厚度、组织特性无法实现有效检测；相控阵超声检测方法能够明显的检测出薄板焊缝奥氏体组织缺陷。

简介：利用CVI法,在两种不同类型的国产SiC纤维束中引入(PyC/SiC)4或(PyC/SiC)8多层界面,并进一步致密化,制备含不同纤维种类和界面类型的SiCf/SiCMini复合材料。研究纤维种类和界面类型对SiCf/SiCMini复合材料力学性能和断裂机制的影响。结果表明:致密化的SiCf/SiCMini复合材料已形成一个整体,在纤维和基体连接处可观察到明显的界面层,且界面厚度均匀;A/(PyC/SiC)4/SiC、B/(PyC/SiC)4/SiC、A/(PyC/SiC)8/SiC三种SiCf/SiCMini复合材料的最大拉伸强度分别达到466,350和330MPa,最终拉伸应变分别达到0.519%,0.219%和0.330%;拉伸断口均有纤维拔出,且随纤维种类或界面类型不同,纤维拔出长度和断口形貌有所差异。其中A/(PyC/SiC)4/SiC以ModelⅡ断裂机制发生断裂,B/(PyC/SiC)4/SiC和A/(PyC/SiC)8/SiC以ModelⅠ断裂机制发生断裂。